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![]() ![]() That is why there are total two signals for compound methyl acetate. The three H b protons in the methyl group bonded with O atom are chemical equivalent as well and show the other signal. All chemical equivalent hydrogens have the same resonance frequency with applied to an external magnetic field, so show only one signal in 1H NMR spectrum. The total six hydrogens can be divided to two groups, the three H a protons in the methyl group that bonded with C=O are all in the same chemical environment, therefore they are chemical equivalent. Why only two signals for a compound containing total six hydrogens? So the compound methyl acetate shows two signals in 1H NMR spectrum. The peak at the far right is for the standard reference compound tetramethylsilane (TMS, more discussions in chemical shift section 6.6.2), not for the compound. 6.6a), we can see that there are three signals. 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